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dc.provenanceCONICET-
dc.creatorOtarola, Jessica Johana-
dc.creatorLista, Adriana Guillermina-
dc.creatorFernández Band, Beatriz Susana-
dc.creatorGarrido, Mariano Enrique-
dc.date2016-03-09T18:31:33Z-
dc.date2016-03-09T18:31:33Z-
dc.date2015-01-
dc.date2016-03-30 10:35:44.97925-03-
dc.date.accessioned2019-04-29T15:30:03Z-
dc.date.available2019-04-29T15:30:03Z-
dc.date.issued2016-03-09T18:31:33Z-
dc.date.issued2016-03-09T18:31:33Z-
dc.date.issued2015-01-
dc.date.issued2016-03-30 10:35:44.97925-03-
dc.identifierOtarola, Jessica Johana; Lista, Adriana Guillermina; Fernández Band, Beatriz Susana; Garrido, Mariano Enrique; Capillary electrophoresis to determine entrapment efficiency of a nanostructured lipid carrier loaded with piroxicam; Elsevier; Journal of Pharmaceutical Analysis; 5; 1; 1-2015; 70-73-
dc.identifier2095-1779-
dc.identifierhttp://hdl.handle.net/11336/4710-
dc.identifier.urihttp://rodna.bn.gov.ar:8080/jspui/handle/bnmm/295261-
dc.descriptionA simple and fast capillary electrophoresis method has been developed to determine the amount of piroxicam loaded in a drug delivery system based on nanostructured lipid carriers (NLC). The entrapment efficiency of the nanostructured lipid carrier was estimated by measuring the concentration of drug not entrapped in a suspension of NLC. The influence of different parameters on migration times, peak symmetry, efficiency and resolution was studied; these parameters included the pH of the electrophoretic buffer solution and the applied voltage. The piroxicam peak was obtained with a satisfactory resolution. The separation was carried out using a running buffer, which it is composed of 50 mmol L-1 ammonium acetate and 13.75 mmol L-1 ammonia at pH 9. The optimal voltage was 20kV and the cartridge temperature was 20°C. The corresponding calibration curve was linear over the range of 2.7 ? 5.4 µg mL-1 of NLC suspension. The reproducibility of migration time and peak area were investigated, and the obtained RSD% values (n = 5) were 0.99 and 2.13, respectively.-
dc.descriptionFil: Otarola, Jessica Johana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Instituto de Química del Sur; Argentina-
dc.descriptionFil: Lista, Adriana Guillermina. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Instituto de Química del Sur; Argentina-
dc.descriptionFil: Fernández Band, Beatriz Susana. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Instituto de Química del Sur; Argentina-
dc.descriptionFil: Garrido, Mariano Enrique. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Bahía Blanca. Instituto de Química del Sur; Argentina-
dc.formatapplication/pdf-
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dc.formatapplication/pdf-
dc.formatapplication/pdf-
dc.languageeng-
dc.publisherElsevier-
dc.relationinfo:eu-repo/semantics/altIdentifier/doi/http://dx.doi.org/10.1016/j.jpha.2014.05.003-
dc.relationinfo:eu-repo/semantics/altIdentifier/url/http://www.sciencedirect.com/science/article/pii/S2095177914000446-
dc.relationinfo:eu-repo/semantics/altIdentifier/issn/2095-1779-
dc.rightsinfo:eu-repo/semantics/openAccess-
dc.rightshttps://creativecommons.org/licenses/by-nc-nd/2.5/ar/-
dc.sourcereponame:CONICET Digital (CONICET)-
dc.sourceinstname:Consejo Nacional de Investigaciones Científicas y Técnicas-
dc.sourceinstacron:CONICET-
dc.source.urihttp://hdl.handle.net/11336/4710-
dc.subjectCAPILLARY ELECTROPHORESIS-
dc.subjectDRUG DELIVERY SYSTEM-
dc.subjectNANOSTRUCTURED LIPID CARRIER-
dc.subjectPIROXICAM-
dc.subjectQuímica Analítica-
dc.subjectCiencias Químicas-
dc.subjectCIENCIAS NATURALES Y EXACTAS-
dc.titleCapillary electrophoresis to determine entrapment efficiency of a nanostructured lipid carrier loaded with piroxicam-
dc.typeinfo:eu-repo/semantics/article-
dc.typeinfo:eu-repo/semantics/publishedVersion-
dc.typeinfo:ar-repo/semantics/articulo-
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